Pilot Reactor System

  • Vessel Capacity: 5L, 10L, 15L, 20L, 50L, 100L
  • Vessel Type: Jacketed and Triple Wall
  • Operating Pressure: Full Vacuum to 0.5 bar G
  • Operating Temperature: -50 °C to 200 °C

Parts

  • Cylindrical Vessel
  • Vessel Cover
  • Quick Release Coupling
  • O-Ring
  • Flush Bottom Valve
  • PTFE Stirrer
  • Man Hole
  • Thermometer Pocket
  • Condenser with reflux
  • Product Cooler
  • Addition Vessel
  • Receiver Vessel
  • Vent
  • Support Structure

Specifications

DESCRIPTION JE-PS-10 JE-KL-20 JE-KL-30 JE-KL-50 JE-KL-100 JE-KL-200 REMARKS / DETAILED DESCRIPTION
GLASS MAIN PARTS
Glass Cylindrical Reactor 10L 20L 30L 50L 100L 200L Option available for Jacketed and Triple Wall (vacuum jacketed) available upto 100L reactor. L/D ratio of the reactor to be maintained.
Top dish N1: DN40 (center nozzle)
N2: DN25 (side nozzle)
N3: DN25 (side nozzle)
N4: DN50 (front nozzle)
N5: DN50 (side nozzle)
N6: DN15 (side nozzle)
N1: DN50 (center nozzle)
N2: DN25 (side nozzle)
N3: DN40 (side nozzle)
N4: DN80 (front nozzle)
N5: DN80 (side nozzle)
N6: DN25 (side nozzle)
N1: DN50 (center nozzle)
N2: DN25 (side nozzle)
N3: DN40 (side nozzle)
N4: DN100 (front nozzle)
N5: DN100 (side nozzle)
N6: DN25 (side nozzle)
Option for SS-PFA lined top dish also available. Nozzle schedule can be modified based on the customer’s requirements.
SS-PTFE Lined Agitator 1 1 1 1 1 1 Option available for Anchor, PBT, CBT impeller in single as well as dual stage. Proper L/D ratio shall be maintained.
Drive assembly for agitator 0.25 HP 0.25 HP 0.5 HP 0.5 HP 1 HP 1 HP Flameproof motor (option available for ATEX certified), gearbox, single mechanical seal (reputed make) and SSPTFE lined agitator.
Glass Feed Vessel 2L 5L 10L 10L 20L 20L Options available in cylindrical as well as spherical vessel, Vessels to be graduated and calibrated
Glass Receiver Vessel 5L 5L 10L 10L 20L 20L Options available in cylindrical as well as spherical vessel. Vessels to be graduated and calibrated
Reflux Divider DN50 DN50 DN80 DN80 DN100 DN150 Option available in manual as well as pneumatic operated automatic relfux divider.
Condenser DN80-C; 0.3 sq.m DN80-C; 0.3 sq.m DN100-C; 0.5 sq.m DN150-C; 1 sq.m DN150-C; 1.5 sq.m DN225-C; 2.5 sq.m C- Coil type condenser
Glass Internal Process Pipelines DN15 / DN25 DN15 / DN25 DN25 DN25 DN25 DN25
Hardware – Plastic flanges, Inserts , SS Nuts, bolts, washers and springs SET SET SET SET SET SET Plastic flanges used as per DIN standard. Option available for SS-304 / SS-316 flanges too.
Structure – Main Frame Suitable size structure to be used. Options available in SS and MS epoxy coated.
SAFETY FEATURES
Rupture Disc DN40 / DN50 DN40 / DN50 DN40 / DN50 DN40 / DN50 DN40 / DN50 DN40 / DN50 Suitable to withstand vacuum and burst pressure rating of 0.6 bar @ 100 DegC.
AUTOMATION AND INSTRUMENTATION
Temperature Sensors 3 3 3 3 3 3 Reactor temp, Reflux temp, Vent temp. Sensor of reputed make (FLP enclosure) Duplex 3 wire Class A PT100 sensors to be used.
Agitator RPM controller (VFD) 1 1 1 1 1 1 Reputed make VFD to be used
Operation & Indication Panel 1 1 1 1 1 1 Option available for :
1) Ex d enclosure (Ex II 2GD Ex DB)
2) PLC with ATEX / NON-ATEX approved HMI.
HMI with PLC panel (Optional) Touchscreen HMI can be provided inside flameproof enclosure along with PLC panel Option available for :
1) Ex d enclosure (Ex II 2GD Ex DB)
2) PLC to be placed in safe area.
SCADA Automation Solution (Optional) PC workstation for controlling, storing and reviewing of process parameters of the assembly. CFR21 PART 11 compliant SCADA automation solutions, pre-defined recipe formulation as per process requirements also available.
ADDITIONAL ACCESSORIES / INFORMATION
Reactor lifting and lowering system Stainless steel lifting and lowering system for reactor vertical movement (up & down) – manual or automatic Used for cleaning and ease of agitator interchangeability
Heating & Cooling System Different models of several temperature ranges and power (kW) are available. Do visit our product page (temperature control unit) for selection of the right model.
Documentation (Optional) SET SET SET SET SET SET Set of documentations and certifications to be provided along with the system.
These are general specifications, it may deviate as per client’s requirement or at detailing stage.
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